Adsorption and reaction of dibromobenzene at the at the Si (111) 7x7 surface

 

1_DBB61A  2_PhBr_SiBr_VertA   3_Ph_2Sigm_Vert

1.   Chemisorption                          2. Br-atom transfer                          3. Second Br-atom transfer

 

Reaction between 1,2-dibromobenzene and the Si(111)-7 [1] 7 surface has been studied theoretically on the

DFT(B3LYP/6-31G(d)) level. A 12-atom silicon cluster, representing two adatoms and one rest atom of the

faulted half of the unit cell, was used to model the silicon surface. The first step of the reaction was a covalent

attachment (chemisorption) of an intact 1,2-dibromobenzene molecule to the silicon cluster. Binding energies

were calculated to be between 1.04 and 1.14 eV, depending on the orientation of the molecule. A second step

of the reaction was the transfer of the Br atom to the silicon cluster. Activation energies for the transfer of

the Br atom were calculated to be between 0.4 and 0.6 eV, suggesting that the thermal bromination reaction

occurs on a microsecond time scale at room temperature. A third step of the reaction could be the transfer of

the second Br atom of the molecule, the desorption of the organic radical, or the change of the adsorption

configuration of the radical, depending on the original orientation of the adsorbed intact molecule. A novel,

aromatic, two-σ-bound adsorbed configuration of the C6H4 radical, in which a carbon ring of the radical is

perpendicular to the silicon surface, has been introduced to explain previous experimental observations (Surf.

Sci. 2004, 561, 11).

 

This work was published in: “An STM study of the localized atomic reaction of 1,2- and 1,4-dibromobenzene at Si (1 1 1)-7 × 7”, S. Dobrin, K.R, Harikumar and J.C. Polanyi, Surface Science, 561 (2004) 11;

"Reaction of 1,2-Dibromobenzene with the Si(111)-7×7 Surface, a DFT Study", S. Dobrin, J. Phys. Chem. B. 109 (2005) 22976